2.2 Methods of Separating & Purifying Substances (Edexcel GCSE Chemistry)

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  • What is the difference between a pure substance and a mixture?

    A pure substance consists of only substance (this can be an element or a compound), while a mixture contains two or more different substances that are not chemically combined.

  • True or False?

    Salt dissolved in water is a pure substance.

    False.

    A solution of salt dissolved in water is a mixture.

  • State what is meant by the term melting point.

    The melting point is the temperature at which a solid turns into a liquid.

  • What is a boiling point?

    The boiling point is the temperature at which a liquid turns into a gas.

  • What property can be used to distinguish a pure substance from a mixture?

    Melting point and boiling point can be used to distinguish a pure substance from a mixture.

  • True or False?

    Pure substances have a range of melting and boiling points.

    False.

    Pure substances have sharp, specific melting and boiling points, while mixtures have a range of melting and boiling points.

  • What is a cooling curve?

    A cooling curve is a graph that shows how a substance changes from a gas to a liquid to a solid as temperature decreases.

  • What does a horizontal line on a cooling curve indicate?

    A horizontal line on a cooling curve indicates where a substance is changing from a gas to a liquid or from a liquid to a solid.

  • What is a pure substance?

    A pure substance is a single element or compound that contains no other substances.

  • How can melting and boiling points distinguish between pure substances and mixtures?

    Pure substances have specific and sharp melting and boiling points, while mixtures have a range of melting and boiling points.

  • State the use of melting point analysis.

    Melting point analysis is used to assess the purity of a substance.

  • X represents the melting point of substances A and B.

    Is substance A pure or impure?

    Line graph showing temperature (°C) over time (seconds), two curves labeled A (black) and B (gray), and a period labeled X. B is lower and intersects A.

    Substance A is impure because it melts over a range of temperatures.

    Line graph showing temperature (°C) over time (seconds), two curves labeled A (black) and B (gray), and a period labeled X. B is lower and intersects A.
  • What does simple distillation separate?

    Simple distillation is used to separate:

    • a liquid and soluble solid from a solution (e.g., water from a solution of salt water)

    • a pure liquid from a mixture of liquids

  • State what is meant by the term simple distillation.

    Simple distillation is a technique used to separate a liquid from a solution (e.g., water from a salt solution) by boiling the solution and condensing the vapour.

  • What is fractional distillation?

    Fractional distillation is a technique used to separate two or more liquids that have different boiling points from a mixture.

  • What does filtration separate?

    Filtration separates an undissolved solid from a mixture of solid and liquid.

  • What is crystallisation used for?

    Crystallisation is used to separate a dissolved solid from a solution.

  • In terms of the solid (solute), what is important about the solvent?

    It is important that the solid (solute) is much soluble in hot solvent than in cold.

  • Which property does paper chromatography depend upon?

    Paper chromatography depends upon the solubility of different substances.

  • What is paper chromatography used for?

    Paper chromatography is used to separate substances that have different solubilities in a given solvent, such as identifying the components of a mixture.

  • What is the mobile phase in paper chromatography?

    The mobile phase in chromatography is the solvent / liquid that travels up the paper.

  • Why should the baseline (starting line) in chromatography be drawn in pencil?

    The baseline (starting line) should be drawn in pencil because it will not contaminate the results / will not run.

  • True or False?

    In paper chromatography, a pure substance produces more than one spot.

    False.

    In paper chromatography, a pure substance only produces one spot.

  • Which technique separates solutions with more than one type of dissolved solid (solute)?

    The technique that separates solutions with more than one type of dissolved solid is chromatography.

  • What does a single spot on a chromatogram indicate?

    A single spot on a chromatogram indicates that the substance is pure.

  • State the equation to calculate the retention factor (Rf value).

    The equation for the retention factor (Rf value) is:

    Rf = fraction numerator Distance space travelled space by space sample over denominator Distance space travelled space by space solvent space front end fraction

  • What does an Rf value closer to 1 indicate?

    An Rf value close to 1 indicates that the component is very / highly soluble in the solvent used.

  • True or False?

    Multiple spots on a chromatogram indicate a pure substance.

    False.

    Multiple spots on a chromatogram indicate that the substance is a mixture.

  • True or False?

    The Rf value of a compound is always the same, regardless of the solvent used.

    False.

    The Rf value of a compound depends on the solvent used.

    If the solvent is changed, the Rf value will change.

  • What is the purpose of calculating Rf values in paper chromatography?

    The purpose of calculating Rf values is to allow chemists to identify unknown substances.

  • What does the Rf value range between?

    The Rf values ranges between 0 and 1.

  • What should the initial line on a chromatogram be drawn with?

    The initial line on a chromatogram should be drawn with a pencil.

  • True or False?

    The solvent level should start above the pencil line on a chromatogram.

    False.

    The solvent level should not start above the pencil line, as this would ruin the chromatogram.

  • How many substances are in sample D?

    Chromatogram

    There are 3 substances in D.

    Chromatogram
  • True or False?

    If two substances are the same, they will produce identical chromatograms.

    True.

    If two substances are the same, they will produce identical chromatograms.

  • Why does an Rf value have no units?

    An Rf value does not have units because it is a ratio.

  • Identify the mobile and stationary phase in the chromatography experiment below.

    Chromatogram 2

    The mobile phase is the water and the stationary phase is the chromatography paper.

    Chromatogram 2
  • Which colours from A-E does black food colouring contain?

    Chromatogram for black ink

    The black food colouring contains A, E and an unknown.

    Chromatogram for black ink
  • What is the first step in the purification water?

    The first step in the purification of water is filtration to remove large particles.

  • What is desalination?

    Desalination is the process of removing salt from seawater to make it suitable for drinking and irrigation.

  • True or False?

    Distillation is used in water purification.

    False.

    Distillation is not used in water purification.

  • What happens during sedimentation in water treatment?

    Sedimentation allows heavy particles to settle at the bottom of the water treatment tanks.

  • What is the purpose of chlorination?

    Chlorination is the process of adding chlorine to water to disinfect it by killing bacteria and other pathogens.

  • True or False?

    Filtration removes dissolved impurities from water.

    False.

    Filtration removes large particles but not dissolved impurities.

  • What is reverse osmosis?

    Reverse osmosis is a water purification process that uses a semi-permeable membrane to remove ions, molecules, and larger particles.

  • Why is deionised water used in chemical analysis?

    Deionised water is used as the ions could react with the substances under analysis and would give the experiment a false result.

  • Why is making sea water potable expensive?

    The process is expensive as a lot of energy is required to heat the large volumes of water to 100 ºC.

  • Define the term potable water.

    Potable water is water that is clean enough for human consumption.