Required Practical 8: Analysis & Purification of Water Samples
Practical 8(a): Analysing and Purifying Water and making it Safe to Drink
Objective
- To determine the amount of dissolved solid in samples of water
Hypothesis
- Analysis of the pH and dissolved solids of water samples can help determine the regions the water comes from
Materials
- Water samples A, B, C and D
- Universal indicator paper
- Mass balance
- Evaporating basin
- 25 cm3 graduated cylinder
- Bunsen burner, tripod & gauze
Practical tip
Don’t overheat during step 4 as you run the risk of thermally decomposing some of the solids, leading to erroneous results
Method
- Use the universal indicator paper to determine the pH of the water sample
- Accurately weigh an empty evaporating basin to two decimal places
- Add 25 cm3 of water sample A into the evaporating basin
- Heat the evaporating basin on a tripod and gauze using a Bunsen burner until the solids start to form and the majority of water has evaporated
- Leave for the remaining water to evaporate off
- Weigh the cooled evaporating basin again and calculate the mass of the solids that were dissolved in the water.
Results
Record your results in a suitable table
| Water sample (20 cm3) | pH | Mass of solid dissolved (g) |
| A | ||
| B |
Evaluation
- The results could be compared to the national water safety levels and by analysis the regions of each sample could be deducted e.g. region of high acid rain, water from a salt water supply etc.
Conclusion
- The amount of dissolved solids in water can be determined and is a useful indicator of water quality
Examiner Tip
Make sure you know the names of common laboratory equipment and can draw and label apparatus used in the required practicals.
Required Practical 8(b): To Purify a Water Sample by Distillation
Objective
- To separate pure clean water from a sample containing water and other substances
Hypothesis
- A simple distillation apparatus can be set up separate pure water from a mixture of water and unwanted substances
Materials
- 10 cm3 of water sample A
- Bunsen burner
- Tripod
- Gauze
- Heatproof mat
- Clamp and clamp stand
- Conical flask with delivery tube and bung
- Boiling tube
- Ice bath
Simple distillation apparatus
Diagram showing the apparatus to set-up for a simple distillation experiment
Practical Tip
The delivery tube must sit above the filtrate level to prevent cold water being sucked back up the delivery tube after separation, which would break the hot glass
Method
- Add the water sample to the conical flask and set up the apparatus for distillation as shown in the diagram
- Heat the water using the Bunsen burner until boiling occurs
- Reduce the heat so that the water boils gently for some time
- The distilled water will collect in the cooled test tube
- Collect about 2 cm depth of water in this way, then stop heating
- Analyse the water you have distilled by determining its boiling point
Results
- Distillate of pure clean water
Evaluation
- The pH of the water can be tested as well as its boiling point
Conclusion
- Simple distillation can be used to produce pure water from a sample of impure or contaminated water
