Synthesis of a Haloalkane (OCR A Level Chemistry)

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PAG 5.1: Synthesis of a Haloalkane

Synthesis of a haloalkane from an alcohol

  • Measure 8 cm3 of 2-methylpropan-2-ol in a measuring cylinder
  • Pour the 2-methylpropan-2-ol into a separating funnel
  • Using a fume hood, add 20 cm3 of concentrated hydrochloric acid to the separating funnel in small portions of 2 - 3 cmmaking sure to release the pressure by opening the stopper after each addition 
  • Leave the separating funnel to stand in the fume hood for 20 minutes and gently shake the separating funnel at 2 minute intervals 
  • Allow the layers to separate and dispose of the lower aqueous layer by opening the tap
  • Add sodium hydrogen carbonate solution in small portions to the funnel and gently shake the funnel, again, release the pressure at regular intervals
    • This removes acidic impurities
  • Once these layers have separated, open the tap once more and dispose of the aqueous layer
  • Pour the organic layer into a clean dry conical flask and add two spatulas of anhydrous magnesium sulfate 
    • This will remove water 
  • Once clear, decant the liquid into distillation apparatus 
  • Distill the liquid and collect the distillate in the range of 47 - 53 oC

Separation of ethyl ethanoate, downloadable AS & A Level Chemistry revision notes

A separating funnel allows the product to be cleaned and isolated

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Philippa

Author: Philippa

Expertise: Chemistry

Philippa has worked as a GCSE and A level chemistry teacher and tutor for over thirteen years. She studied chemistry and sport science at Loughborough University graduating in 2007 having also completed her PGCE in science. Throughout her time as a teacher she was incharge of a boarding house for five years and coached many teams in a variety of sports. When not producing resources with the chemistry team, Philippa enjoys being active outside with her young family and is a very keen gardener.