Making Simple Cells (AQA A Level Chemistry)

Revision Note

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Stewart Hird

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Making Simple Cells

  • Simple cells can be used to investigate the effect of different electrode combinations on the EMF produced by an electrochemical cell

Key steps in the procedure

  • The metal foil electrodes are cleaned using sandpaper and rinsed under a cold running tap

  • The metal foil is immersed into a solution of its ions and can be secured in place by folding the end over the lip of the beaker

  • A strip of filter paper is soaked in saturated potassium chloride or nitrate solution to form the salt bridge; the ends of the strip are then immersed in metal ion solutions

  • The EMF of the cells can then be measured and compared to the expected voltage from standard electrode potentials

Electrochemistry Calculations - Electrochemical Cell, downloadable AS & A Level Chemistry revision notes

Measuring the EMF of different metal electrode combinations

Measured EMF specimen results table

Metals and emf specimen results, downloadable AS & A Level Chemistry revision notes

 

  • Measured results in the lab are generally lower than calculated results from data tables

  • This is usually because non-standard conditions have been used

Examiner Tips and Tricks

An electrode always contains a metal in contact with a solution of its own ions.By convention, EMF values are positive and the more negative electrode is written on the left.When calculating the EMF, subtract the right-hand electrode potential from the left hand one.Electrode equations are always written as reduction processes 

Changing Conditions in Simple Cells

  • The same procedure as the previous experiment can be used to investigate the effect of concentration on the EMF of an electrochemical cell

  • At the end of the first measurement one of the solutions is diluted by a factor of ten by taking 25 cm3 of the solution and diluting it to 250 cm3 with distilled water using a large measuring cylinder

  • The EMF is measured and the process is repeated until a total of five dilutions have been carried out

Practical tip

  • Although in principle any pair of metals be used its best to use metals with a sufficiently large difference in electrode potential for this experiment so the range of results in meaningful

Concentration and EMF specimen results table

Concentration and emf specimen results, downloadable AS & A Level Chemistry revision notes

 

Analysis

  • A graph can be plotted of EMF versus dilution factor:

 

Concentration and emf graph, downloadable AS & A Level Chemistry revision notes

Graph of EMF against dilution for an electrochemical cell

  • The graph shows that the cell EMF is proportional to the dilution to the power of ten

  • Decreasing the concentration of the solution reduces the cell EMF because there are fewer particles to react

Further investigations

  • The same equipment can be used to investigate the effect on cell EMF of changing the temperature, the spacing between the electrodes and even the depth of the electrodes

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Stewart Hird

Author: Stewart Hird

Expertise: Chemistry Lead

Stewart has been an enthusiastic GCSE, IGCSE, A Level and IB teacher for more than 30 years in the UK as well as overseas, and has also been an examiner for IB and A Level. As a long-standing Head of Science, Stewart brings a wealth of experience to creating Topic Questions and revision materials for Save My Exams. Stewart specialises in Chemistry, but has also taught Physics and Environmental Systems and Societies.